The Role of Energy Density in Phase-Microstructure Evolution and Mechanical Properties of Ti-Zr-Cu Alloys Fabricated by Laser Powder-Bed Fusion

Authors

  • Pattarapong Wannapraphai Chulalongkorn University
  • Thanawat Phetrattanarangsi Chulalongkorn University
  • Surasak Kuimalee Maejo University
  • Boonrat Lohwongwatana Chulalongkorn University
  • Chedtha Puncreobutr Chulalongkorn University

DOI:

https://doi.org/10.4186/ej.2024.28.12.101

Keywords:

laser powder-bed fusion, Ti-Zr-Cu alloys, energy density, microstructure evolution, hardness

Abstract

Laser powder-bed fusion (L-PBF) additive manufacturing technique offers significant advantages in fabricating Ti-Zr-Cu alloys by enabling precise control over microstructure through process parameter variation. This study investigates the impact of energy density on phase formation, microstructure evolution, and mechanical properties of Ti-Zr-Cu alloys produced from blended elemental powders. By adjusting laser scan speeds to achieve different energy densities, the study reveals that high energy densities result in homogeneous β-(Ti,Zr) phases, while lower energy densities lead to incomplete melting, phase segregation, and inhomogeneous microstructures. Advanced characterisation techniques, including scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD), were utilised to analyse phase composition and microstructural transformations. Vickers hardness testing demonstrated a correlation between energy density and mechanical properties, with higher energy densities improving overall material hardness. The findings offer valuable insights into optimising L-PBF process parameters for enhanced performance in additively manufactured Ti-Zr-Cu alloys, providing a pathway for advanced applications in biomedical and structural components.

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Author Biographies

Pattarapong Wannapraphai

Laser powder-bed fusion (L-PBF) additive manufacturing technique offers significant advantages in fabricating Ti-Zr-Cu alloys by enabling precise control over microstructure through process parameter variation. This study investigates the impact of energy density on phase formation, microstructure evolution, and mechanical properties of Ti-Zr-Cu alloys produced from blended elemental powders. By adjusting laser scan speeds to achieve different energy densities, the study reveals that high energy densities result in homogeneous β-(Ti,Zr) phases, while lower energy densities lead to incomplete melting, phase segregation, and inhomogeneous microstructures. Advanced characterisation techniques, including scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD), were utilised to analyse phase composition and microstructural transformations. Vickers hardness testing demonstrated a correlation between energy density and mechanical properties, with higher energy densities improving overall material hardness. The findings offer valuable insights into optimising L-PBF process parameters for enhanced performance in additively manufactured Ti-Zr-Cu alloys, providing a pathway for advanced applications in biomedical and structural components.

Thanawat Phetrattanarangsi

Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, 10330, Thailand

Surasak Kuimalee

Industrial Chemistry Innovation Programme, Faculty of Science, Maejo University, Chiang Mai 50290, Thailand

Boonrat Lohwongwatana

Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, 10330, Thailand

Chedtha Puncreobutr

Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, 10330, Thailand

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Published In
Vol 28 No 12, Dec 31, 2024
How to Cite
[1]
P. Wannapraphai, T. Phetrattanarangsi, S. Kuimalee, B. Lohwongwatana, and C. Puncreobutr, “The Role of Energy Density in Phase-Microstructure Evolution and Mechanical Properties of Ti-Zr-Cu Alloys Fabricated by Laser Powder-Bed Fusion ”, Eng. J., vol. 28, no. 12, pp. 101-110, Dec. 2024.

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